Alphacypermethrin residues in milk following a pour-on treatment in buffaloes


https://doi.org/10.4081/ijfs.2013.960
Vol. 2 No. 2 (2013)
Submitted: 15 January 2013
Accepted: 15 April 2013
Published: 10 June 2013
Alphacypermethrin, Buffaloes, Milk, Pour-on treatment
Abstract Views: 921
PDF: 1083
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Authors

  • Giorgio Smaldone
    giorgio.smaldone@unina.it
    Dipartimento di Scienze zootecniche ed Ispezione degli alimenti, Università degli studi di Napoli “Federico II”, Facoltà di Medicina Veterinaria, Napoli, Italy.
  • Raffaele Marrone Dipartimento di Scienze zootecniche ed Ispezione degli alimenti, Università degli studi di Napoli “Federico II”, Facoltà di Medicina Veterinaria, Napoli, Italy.
  • Claudia Chirollo Dipartimento di Scienze zootecniche ed Ispezione degli alimenti, Università degli studi di Napoli “Federico II”, Facoltà di Medicina Veterinaria, Napoli, Italy.
  • Lucia Vollano Dipartimento di Scienze zootecniche ed Ispezione degli alimenti, Università degli studi di Napoli “Federico II”, Facoltà di Medicina Veterinaria, Napoli, Italy.
  • Raffaella Mercogliano Dipartimento di Scienze zootecniche ed Ispezione degli alimenti, Università degli studi di Napoli “Federico II”, Facoltà di Medicina Veterinaria, Napoli, Italy.
  • Aniello Anastasio Dipartimento di Scienze zootecniche ed Ispezione degli alimenti, Università degli studi di Napoli “Federico II”, Facoltà di Medicina Veterinaria, Napoli, .
Aim of this study was to detect and quantify the residues of alphacypermethrin (ACYP), a pyrethroid insecticide, in buffalo milk. Ten animals were treated pour-on at the manufacturer’s recommended cattle dose. Milk samples were collected from each animal before treatment, every 12 h for the first three days (12, 24, 36, 48, 60, 72 h) and once on day 5 after treatment. Milk samples were subsequently analysed by ultraperformance liquid chromatography coupled with tandem mass spectrometry (UPLC-MS/MS). All samples showed levels of ACYP above the maximum residual limit of 20 ppb established for bovine milk.

1.
Smaldone G, Marrone R, Chirollo C, Vollano L, Mercogliano R, Anastasio A. Alphacypermethrin residues in milk following a pour-on treatment in buffaloes. Ital J Food Safety [Internet]. 2013 Jun. 10 [cited 2024 Apr. 19];2(2):e19. Available from: https://www.pagepressjournals.org/ijfs/article/view/ijfs.2013.e19

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